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a–c PDF G(r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 O–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , hcp-LZC, and 0.8Li 2 O–ZrCl 4 . <t>e</t> <t>HRTEM</t> image with <t>FFT</t> patterns of 0.8Li 2 O–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).
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a–c PDF G(r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 O–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , hcp-LZC, and 0.8Li 2 O–ZrCl 4 . <t>e</t> <t>HRTEM</t> image with <t>FFT</t> patterns of 0.8Li 2 O–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).
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a–c PDF G(r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 O–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , hcp-LZC, and 0.8Li 2 O–ZrCl 4 . e HRTEM image with FFT patterns of 0.8Li 2 O–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).

Journal: Nature Communications

Article Title: Divalent anion-driven framework regulation in Zr-based halide solid electrolytes for all-solid-state batteries

doi: 10.1038/s41467-025-65702-2

Figure Lengend Snippet: a–c PDF G(r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 O–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , hcp-LZC, and 0.8Li 2 O–ZrCl 4 . e HRTEM image with FFT patterns of 0.8Li 2 O–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).

Article Snippet: For the HRTEM measurements, the samples were loaded onto a lacey Cu grid in an Ar-filled glove box, and HRTEM images with FFT patterns were obtained using a JEM-ARM 300 F NEOARM (JEOL).

Techniques:

a–c , PDF G (r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 S–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , ccp-LZC, and 0.8Li 2 S–ZrCl 4 . e HRTEM image with FFT patterns of 0.8Li 2 S–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).

Journal: Nature Communications

Article Title: Divalent anion-driven framework regulation in Zr-based halide solid electrolytes for all-solid-state batteries

doi: 10.1038/s41467-025-65702-2

Figure Lengend Snippet: a–c , PDF G (r) ( a ) normalized Zr K-edge XANES spectra ( b ) and Zr K-edge EXAFS spectra ( c ) of x Li 2 S–ZrCl 4 ( x = 0.6, 0.8, 1.0, 1.2, 1.6, 2.0). d Raman spectra for ZrCl 4 , ccp-LZC, and 0.8Li 2 S–ZrCl 4 . e HRTEM image with FFT patterns of 0.8Li 2 S–ZrCl 4 (scale bar: 20 nm) with corresponding FFT patterns (scale bar: 2 nm⁻¹).

Article Snippet: For the HRTEM measurements, the samples were loaded onto a lacey Cu grid in an Ar-filled glove box, and HRTEM images with FFT patterns were obtained using a JEM-ARM 300 F NEOARM (JEOL).

Techniques: